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Kathy Keithley-Johnston kkjohnston@toxicdiscovery.com

25 septembre, 2005 15:14

We are the Evidence 3

Shanklin and Smalley in TN. do some wonderful research concerning this. I have attached a sample showing silicone. My spinal fluid was reviewed this way and did show a close match to Dow. My Mfgs. was H/S but my silicone was Dow.

Our Organization suggests this type of testing to prove that one's silicone from their implant migrated into the tissue that is being tested.

Kathy

Kathy L. Keithley-Johnston, R.N.
Executive Director

Toxic Discovery
601 W. Nifong - Bldg. 3B. - Suite P.
Columbia, MO. 65203

Phone: 573.817.2090
Fax: 573.445.4700

"Informed Consent Begins With Informed Individuals"

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Sent: Sunday, September 25, 2005 12:26 PM

Subject: Re: We are the Evidence

Hi, everyone... Hope this finds you well..

Kathy or anyone, Do you know what labs we can trust? So many of us are getting shafted on our reports! I have tested postive for Lupus years ago but then the reports deny the lab reports from the past and even Dr. Vasey says its not worth retesting!! Grrrr

Hope everyone is enjoying the weekend!

Hugs, Rosie =)

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Fourier Transform Infrared Spectroscopy (FTIR) is a powerful tool for identifying types of chemical bonds in a molecule by producing an infrared absorption spectrum that is like a molecular "fingerprint".

FTIR - Introduction

FTIR is most useful for identifying chemicals that are either organic or inorganic. It can be utilized to quantitate some components of an unknown mixture. It can be applied to the analysis of solids, liquids, and gasses. The term Fourier Transform Infrared Spectroscopy (FTIR) refers to a fairly recent development in the manner in which the data is collected and converted from an interference pattern to a spectrum. Today's FTIR instruments are computerized which makes them faster and more sensitive than the older dispersive instruments.

Qualitative Analysis

FTIR can be used to identify chemicals from spills, paints, polymers, coatings, drugs, and contaminants. FTIR is perhaps the most powerful tool for identifying types of chemical bonds (functional groups). The wavelength of light absorbed is characteristic of the chemical bond as can be seen in this annotated spectrum.

By interpreting the infrared absorption spectrum, the chemical bonds in a molecule can be determined. FTIR spectra of pure compounds are generally so unique that they are like a molecular "fingerprint". While organic compounds have very rich, detailed spectra, inorganic compounds are usually much simpler. For most common materials, the spectrum of an unknown can be identified by comparison to a library of known compounds. WCAS has several infrared spectral libraries including on-line computer libraries. To identify less common materials, IR will need to be combined with nuclear magnetic resonance, mass spectrometry, emission spectroscopy, X-ray diffraction, and/or other techniques.

Quantitative Analysis

Because the strength of the absorption is proportional to the concentration, FTIR can be used for some quantitative analyses. Usually these are rather simple types of tests in the concentration range of a few ppm up to the percent level. For example, EPA test methods 418.1 and 413.2 measure the C-H absorption for either petroleum or total hydrocarbons. The amount of silica trapped on an industrial hygiene filter is determined by FTIR using NIOSH method 7602.

Physical Principles

Molecular bonds vibrate at various frequencies depending on the elements and the type of bonds. For any given bond, there are several specific frequencies at which it can vibrate. According to quantum mechanics, these frequencies correspond to the ground state (lowest frequency) and several excited states (higher frequencies). One way to cause the frequency of a molecular vibration to increase is to excite the bond by having it absorb light energy. For any given transition between two states the light energy (determined by the wavelength) must exactly equal the difference in the energy between the two states [usually ground state (E0) and the first excited state (E1)].

 

 


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